A peptide solution was scanned using a high sensitivity DSC and showed no signs of secondary structure.

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Zn+2 was injected into the peptide solution at a number of temperatures.  The kinetics of crystallization were monitored in real time.
 

The peptide-Zn+2 solutions were scanned in a HSDSC.  Note the endothermic process associated with disruption of the complex and exothermic peak possibly caused by aggregation.